Study on Synthesis and Characterization of Hexaquonickel(II) bis-p-toluenesulfonate

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Published Aug 16, 2017
DOI https://doi.org/10.9734/AJOCS/2017/35519
    Page: 1-8

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Wu Shutian
Institute of Chemical Engineering, East China University of Science and Technology, 200237, Shanghai, China
Zhu Qinyu
Institute of Chemical Engineering, East China University of Science and Technology, 200237, Shanghai, China
Guo Wenhui
Institute of Chemical Engineering, East China University of Science and Technology, 200237, Shanghai, China
Xiong Wanli
Institute of Chemical Engineering, East China University of Science and Technology, 200237, Shanghai, China
Tang Shiyi
Institute of Chemical Engineering, East China University of Science and Technology, 200237, Shanghai, China
Xue Weilan
Institute of Chemical Engineering, East China University of Science and Technology, 200237, Shanghai, China
Zeng Zuoxiang
Institute of Chemical Engineering, East China University of Science and Technology, 200237, Shanghai, China

Abstract

Hexaquonickel (II) bis-p-toluenesulfonate [Ni(OTs)2·6H2O] was prepared from the reaction of p-toluenesulfonic acid (PTS) and nickel hydroxide [Ni(OH)2]. Energy disperse spectroscopy, thermal-analysis instrument, infrared spectrometer, and X-ray diffractometer were used to characterize the product of Ni(OTs)2·6H2O purified by recrystallization. The influence of equivalence ratio of reactants [NPTS/NNi(OH)2], reaction temperature and reaction time on the yield of products was investigated. The results show that when the value of NPTS/NNi(OH)2 is 1.1, reaction temperature is 353 K, and reaction time is 3 h, the yield of the product is 90.86%.

Keywords:
Hexaquonickel (II) bis-p-toluenesulfonate, synthesis, characterization, yield

Article Details

How to Cite
Shutian, W., Qinyu, Z., Wenhui, G., Wanli, X., Shiyi, T., Weilan, X., & Zuoxiang, Z. (2017). Study on Synthesis and Characterization of Hexaquonickel(II) bis-p-toluenesulfonate. Asian Journal of Chemical Sciences, 3(2), 1-8. https://doi.org/10.9734/AJOCS/2017/35519
Issue
2017 - Volume 3 [Issue 2]
Section
Original Research Article